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CAM Workgroup: Work Products

Cleanup of Sites & Spills: CAM Workgroup: Work Products
Introduction

The following documents are revisions of recommended laboratory procedures and field sample Quality Assurance/Quality Control (QA/QC) requirements for analytical data used in support of assessment and evaluation decisions at disposal sites regulated under M.G.L.c. 21E, the Massachusetts Contingency Plan (MCP).

Comments and recommendations on these revisions should be directed to:
Donald Muldoon
Massachusetts Department of Environmental Protection
One Winter Street Boston, MA 02108
(617) 292 - 5785
donald.muldoon@state.ma.us

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
I Overview

Overview of the MCP Analytical Data Enhancement Process

Draft Revision 1
October 15, 2009
MS Word 770 KB | PDF 265 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
II Gas Chromatography/Mass Spectrometric (GC/MS) Methods

A. QA/QC Requirements and Performance Standards for SW-846 Method 8260B, Volatile Organics by GC/MS

Draft Revision 1
September 8, 2009
MS Word 1.1 MB | PDF 317 KB

B. QA/QC Requirements and Performance Standards for SW-846 Method 8270D, Semi-Volatile Organics by GC/MS 

Draft Revision 1
September 9, 2009
MS Word 609 KB | PDF 388 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
III Metal Analysis

A. QA/QC Requirements and Performance Standards for SW-846 Method 6010C, Trace Metals by ICP-AES

Draft Revision 1
November 9, 2009
MS Word 724 KB | PDF 342 KB

B. QA/QC Requirements and Performance Standards for SW-846 Methods 7470/7471, Mercury by Cold Vapor AAS

Draft Revision 1
October 30, 2009
MS Word 439 KB | PDF 253 KB

C. QA/QC Requirements and Performance Standards for SW-846 Method 7010, Trace Metals by GFAA

Draft Revision 1
November 16, 2009
MS Word 628 KB | PDF 327 KB

D. QA/QC Requirements and Performance Standards for SW-846 Method 6020A, Trace Metals by ICP-MS

Draft Revision 1
November 10, 2009
MS Word 791 KB | PDF 350 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
IV Petroleum Hydrocarbon Methods

A. Method and QA/QC Requirements and Performance Standards for Volatile Petroleum Hydrocarbons (MADEP-VPH-04-1.1) 

Draft Revision 1
September 17, 2009
MS Word 944 KB | PDF 402 KB

B. Method and QA/QC Requirements and Performance Standards for Extractable Petroleum Hydrocarbons (MADEP-EPH-04-1.1)

Draft Revision 1
September 16, 2009
MS Word 981 KB | PDF 1.2 MB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
V Gas Chromatographic Methods

A. QA/QC Requirements and Performance Standards for SW-846 Method 8082A, Polychlorinated Biphenyls (PCBs)

Draft Revision 1
September 14, 2009
MS Word 609 KB | PDF 388 KB

B. QA/QC Requirements and Performance Standards for SW-846 Method 8081B, Chlorinated Pesticides

Draft Revision 1
September 10, 2009
MS Word 614 KB | PDF 301 KB

C. QA/QC Requirements and Performance Standards for SW-846 Method 8151A, Chlorinated Herbicides

Draft Revision 1
September 18, 2009
MS Word 588 KB | PDF 324 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
VI Miscellaneous Wet Chemical Methods

A. Quality Control Requirements and Performance Standards for the Analysis of Total Cyanide and Physiologically Available Cyanide (PAC)

Draft Revision 1
November 13, 2009
MS Word 588 KB | PDF 323 KB

B. QA/QC Requirements and Performance Standards for SW-846 Method 7196A, Hexavalent Chromium

Not yet available

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
VII Sampling, Data Evaluation, and Reporting

QA/QC Guidelines for the Acquisition and Reporting of Analytical Data

Draft Revision 1
October 15, 2009
MS Word 2 MB | PDF 682 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
VIII High Performance Liquid Chromatography (HPLC) Methods

A. QA/QC Requirements and Performance Standards for SW-846 Method 8330A, Nitroaromatics and Nitramines

Draft Revision 1
Novwember 13, 2009
MS Word 657 KB | PDF 363 KB

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Cleanup of Sites & Spills: CAM Workgroup: Work Products
IX Air Sampling Methods

A.  QA/QC Requirementsand Performance Standards for the Analysis of Air-Phase Petroleum Hydrocarbons (APH) by Gas Chromatography/Mass Spectrometry

Draft Revision 0
November 5, 2009
MS Word 260 KB | PDF 822 KB

B.  QA/QC Requirementsand Performance Standards for the Analysis of Volatile Organic Compounds in Air Samples (TO-15) by Gas Chromatography/Mass Spectrometry

Draft Revision 0
November 9, 2009
MS Word 996 KB | PDF 355 KB

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